Synthesis and Properties of thermally Reduced Graphene Oxide/Polyacrylonitrile Composites

Title
Synthesis and Properties of thermally Reduced Graphene Oxide/Polyacrylonitrile Composites
Authors
이성호김양진김도환구본철조한익
Keywords
Polymers; Differential scanning calorimetry (DSC); DSC; Infrared spectroscopy; Electrical properties
Issue Date
2012-06
Publisher
The Journal of physics and chemistry of solids
Citation
VOL 73, NO 6, 741-743
Abstract
Graphene oxide (GO) was prepared from graphite using a modified Hummers method. The GO dispersed in dimethyl sulfoxide (DMSO) was incorporated into polyacrylonitrile (PAN) dissolved in DMSO to prepare composite films using a conventional solution-casting method. DSC results showed a significant decrease in the cyclization temperature of polyacrylonitrile (PAN) in the presence of GO because the functional groups of GO initiated cyclization at lower temperature by an ionic mechanism. Heat treatment in air at 250 °C for 3 h led to stabilization of PAN and a simultaneous partial reduction of GO. A significant decrease in the electrical resistivity of the GO/PAN composite films was observed because the partially reduced GO acted as a conducting filler.
URI
http://pubs.kist.re.kr/handle/201004/43653
ISSN
00223697
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KIST Publication > Article
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