Synthesis and characterization of DyxCo1-xFe2-xO4 nanoparticles

Title
Synthesis and characterization of DyxCo1-xFe2-xO4 nanoparticles
Authors
채근화Jitendra Pal SinghHemaunt KumarR.C. SrivastavaK.R. Patel
Keywords
Nanoparticles; Raman spectroscopy; Moessbauer spectroscopy; Magnetic materials
Issue Date
2017-09
Publisher
Superlattices and microstructures
Citation
VOL 109-306
Abstract
In the present work, we report the synthesis of Dy doped CoFe2O4 nanoparticles using chemical method. Doping of Dy ions upto 0.15 in the host lattice does not result into impurity phase as revealed from X-ray diffraction (XRD) and Raman spectroscopy measurments. Near edge X-ray absorption fine structure measurments show the modification of Fe(3d)-O(2p) states and onset of 3+ valence state of Dy ions. Rietveld Refinment of XRD patterns, Mö ssbauer spectroscopy and Fe K-edge extended X-ray absorption fine structure measurments show cation reditribution after doping with Dy ions. All the synthesized nanoparticles exhibit ferrimagnetic like behavior. Coercivity increases with Dy doping concentration. Variation of saturation magnetization with Dy concentration is explained on the basis of cation redistribution and size effect.
URI
http://pubs.kist.re.kr/handle/201004/66184
ISSN
0749-6036
Appears in Collections:
KIST Publication > Article
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