Gujar, T. P. Kim, Woo-Young Jung, Kwang-Deog Joo, Oh-Shim 2024-01-20T23:32:53Z 2024-01-20T23:32:53Z 2021-08-31 2008-04 0013-4651 https://pubs.kist.re.kr/handle/201004/133618 A porous, weblike network with a compact layer of InSe was fabricated on tin-doped indium oxide (ITO) coated glass substrate by the electrodeposition method from an aqueous acidic bath at room temperature. The crystal structure and stoichiometry were studied by X-ray diffraction (XRD) and energy-dispersive analysis by X-ray (EDAX) spectrums, respectively. The nucleation and growth mechanism was studied from cross-sectional and surface-view scanning electron microscopy images. XRD studies of electrodeposited InSe films reveal monoclinic and rhombohedral structures, and the EDAX spectrum confirmed the stoichiometry in the ratio of In:Se=48:52. Surface observations of produced films show a weblike network structure covering the compact layer of InSe. A compact layer is indeed initially formed onto the ITO, and seeds start to grow by a nucleation and growth mechanism. The elemental surface analysis of the core-shell nanoparticles determined by X-ray photoelectron spectroscopy confirmed the chemical nature of the material. (c) 2008 The Electrochemical Society. English ELECTROCHEMICAL SOC INC SELENIDE THIN-FILMS CHEMICAL-VAPOR-DEPOSITION ELECTROCHEMICAL SYNTHESIS SOLAR-CELLS INDIUM GROWTH NANOPARTICLES SPECTROSCOPY SUBSTRATE Porous weblike network of InSe on a compact layer by electrodeposition Article 10.1149/1.2898883 1 JOURNAL OF THE ELECTROCHEMICAL SOCIETY, v.155, no.6, pp.E57 - E62 JOURNAL OF THE ELECTROCHEMICAL SOCIETY 155 6 E57 E62 scie scopus 000255524100040 2-s2.0-43049110626 Electrochemistry Materials Science, Coatings & Films Electrochemistry Materials Science Article SELENIDE THIN-FILMS CHEMICAL-VAPOR-DEPOSITION ELECTROCHEMICAL SYNTHESIS SOLAR-CELLS INDIUM GROWTH NANOPARTICLES SPECTROSCOPY SUBSTRATE