PIOTTO, ME GRANGER, JN CHO, Y FARSCHTSCHI, N GORENSTEIN, DG 2024-01-21T23:45:23Z 2024-01-21T23:45:23Z 2021-08-31 1991-04-08 0040-4020 https://pubs.kist.re.kr/handle/201004/146810 Thiophosphoramidite as well as thiophosphoramidate chemistry has been used to prepare dithiophosphate analogues of oligonucleotides. The H-1 and P-31 resonances of the 3'-thymidine phosphorodithioate decamer d(CGCTpS-2TpS-2AAGCG) were assigned by two-dimensional NMR and the solution structure determined. English PERGAMON-ELSEVIER SCIENCE LTD PURE-ABSORPTION-PHASE RELAXATION MATRIX APPROACH OVERHAUSER EFFECT SPECTRA DINUCLEOSIDE PHOSPHORODITHIOATES DEOXYNUCLEOSIDE PHOSPHORAMIDITES OLIGODEOXYRIBONUCLEOSIDE METHYLPHOSPHONATES PROTON RESONANCES P-31 SIGNALS ASSIGNMENT DEOXYOLIGONUCLEOTIDES SYNTHESIS, NMR AND STRUCTURE OF OLIGONUCLEOTIDE PHOSPHORODITHIOATES Article 10.1016/S0040-4020(01)81780-4 1 TETRAHEDRON, v.47, no.14-15, pp.2449 - 2461 TETRAHEDRON 47 14-15 2449 2461 scie scopus A1991FB16500009 Chemistry, Organic Chemistry Article PURE-ABSORPTION-PHASE RELAXATION MATRIX APPROACH OVERHAUSER EFFECT SPECTRA DINUCLEOSIDE PHOSPHORODITHIOATES DEOXYNUCLEOSIDE PHOSPHORAMIDITES OLIGODEOXYRIBONUCLEOSIDE METHYLPHOSPHONATES PROTON RESONANCES P-31 SIGNALS ASSIGNMENT DEOXYOLIGONUCLEOTIDES oligonucleotide phosphorodithioates ³¹p NMR spectroscopy