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A Concise Synthesis of Tetrabenazine: An Intramolecular Aza-Prins-Type Cyclization via Oxidative C-H Activation

Authors
Son, Young Wook; Kwon, Tae Hui; Lee, Jae Kyun; Pae, Ae Nim; Lee, Jae Yeol; Cho, Yong Seo; Min, Sun-Joon
Issue Date
2011-12-16
Publisher
AMER CHEMICAL SOC
Citation
ORGANIC LETTERS, v.13, no.24, pp.6500 - 6503
Abstract
A concise synthesis of tetrabenazine and dihydrotetrabenazine is described. The key feature of this synthesis is the intramolecular aza-Prins-type cyclization of an amino allylsilane via oxidative C-H activation.
Keywords
VESICULAR MONOAMINE TRANSPORTER; CARBON BOND FORMATION; DIHYDROTETRABENAZINE; (+)-ALPHA-DIHYDROTETRABENAZINE; ALLYLSILANES; CATALYST; DISEASE; ESTERS; AGENT; DDQ; VESICULAR MONOAMINE TRANSPORTER; CARBON BOND FORMATION; DIHYDROTETRABENAZINE; (+)-ALPHA-DIHYDROTETRABENAZINE; ALLYLSILANES; CATALYST; DISEASE; ESTERS; AGENT; DDQ
ISSN
1523-7060
URI
https://pubs.kist.re.kr/handle/201004/129712
DOI
10.1021/ol202792q
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KIST Article > 2011
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