Effects of β-SiC particle seeds on morphology and size of high purity β-SiC powder synthesized using sol-gel process

Authors
Kim, G.-M.Cho, G.-S.Park, S.-W.
Issue Date
2009-09
Citation
Journal of the Korean Ceramic Society, v.46, no.5, pp.528 - 533
Abstract
High purity β-SiC powders were synthesized using sol-gel processing. TEOS and phenol resin were used as the starting material for the silicon source and carbon source, respectively. The process turned out to be capable of producing high purity SiC powder purity degree with 99.98 %. However, it was difficult to control the shape and size of β-SiC powders synthesized by sol-gel process. In this study, β-SiC powder with size of 1∼5 um an 30 nm were used as the seeds for β-SiC to control the β-SiC powder morphology. It was found that β-SiC powder seeds was effective to increase the powder average size of synthesized β-SiC using sol-gel process by acting as the preferred growing sites for β-SiC.
Keywords
Average size; Carbon source; High purity; High purity powders; High-purity SiC; Morphology and size; Phenol resin; Shape and size; SiC particles; SiC powder; Sol-Gel processing; Starting materials; Gels; Morphology; Nanostructured materials; Phenolic resins; Phenols; Resins; Seed; Silicon carbide; Sol-gels; Sols; Synthesis (chemical); Sol-gel process; Average size; Carbon source; High purity; High purity powders; High-purity SiC; Morphology and size; Phenol resin; Shape and size; SiC particles; SiC powder; Sol-Gel processing; Starting materials; Gels; Morphology; Nanostructured materials; Phenolic resins; Phenols; Resins; Seed; Silicon carbide; Sol-gels; Sols; Synthesis (chemical); Sol-gel process; β-sic; High purity; Powder; Seeds; Sol-gel process; Synthesis of sic
ISSN
1229-7801
URI
https://pubs.kist.re.kr/handle/201004/132220
DOI
10.4191/KCERS.2009.46.5.528
Appears in Collections:
KIST Article > 2009
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