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dc.contributor.authorHan, KR-
dc.contributor.authorKim, CS-
dc.contributor.authorKwon, YS-
dc.date.accessioned2024-01-21T03:06:19Z-
dc.date.available2024-01-21T03:06:19Z-
dc.date.created2021-09-01-
dc.date.issued2006-04-01-
dc.identifier.issn0040-6031-
dc.identifier.urihttps://pubs.kist.re.kr/handle/201004/135595-
dc.description.abstractPb(OH)(2) was previously proposed as an intermediate in the synthesis of PMN [Pb(Mg1/3Nb2/3)O-3] and PMN-PT [0.9Pb(Mg1/3Nb2/3)O-3-0.1PbTiO(3)] from a mixture of PbO, Nb2O5, Mg(NO3)(2)(.)6H(2)O (w/w(0)) TiO2 by the modified mixed oxide method based on TG/DSC and XRD data. Coupled TG-MS of the precursor reveals that the intermediate is Pb6O5(NO3)(2), not Pb(OH)(2) because the evolved gas was nitric oxide and oxygen, not water. (c) 2005 Elsevier B.V. All rights reserved.-
dc.languageEnglish-
dc.publisherELSEVIER-
dc.subjectLEAD-MAGNESIUM NIOBATE-
dc.subjectDIELECTRIC-PROPERTIES-
dc.subjectCERAMICS-
dc.subjectMICROSTRUCTURE-
dc.subjectPOWDER-
dc.subjectOXIDE-
dc.titleCoupled TG-MS study on the intermediate for formation of PbO(t) from PbO(O) in synthesis of perovskite PMN-PT-
dc.typeArticle-
dc.identifier.doi10.1016/j.tca.2005.11.040-
dc.description.journalClass1-
dc.identifier.bibliographicCitationTHERMOCHIMICA ACTA, v.443, no.1, pp.122 - 124-
dc.citation.titleTHERMOCHIMICA ACTA-
dc.citation.volume443-
dc.citation.number1-
dc.citation.startPage122-
dc.citation.endPage124-
dc.description.journalRegisteredClassscie-
dc.description.journalRegisteredClassscopus-
dc.identifier.wosid000236644800015-
dc.identifier.scopusid2-s2.0-33644952223-
dc.relation.journalWebOfScienceCategoryThermodynamics-
dc.relation.journalWebOfScienceCategoryChemistry, Analytical-
dc.relation.journalWebOfScienceCategoryChemistry, Physical-
dc.relation.journalResearchAreaThermodynamics-
dc.relation.journalResearchAreaChemistry-
dc.type.docTypeArticle-
dc.subject.keywordPlusLEAD-MAGNESIUM NIOBATE-
dc.subject.keywordPlusDIELECTRIC-PROPERTIES-
dc.subject.keywordPlusCERAMICS-
dc.subject.keywordPlusMICROSTRUCTURE-
dc.subject.keywordPlusPOWDER-
dc.subject.keywordPlusOXIDE-
dc.subject.keywordAuthoroxide-
dc.subject.keywordAuthorchemical synthesis-
dc.subject.keywordAuthordifferential scanning calorimetry-
dc.subject.keywordAuthorthermogravimetric analysis-
dc.subject.keywordAuthorferroelectricity-
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