Effects of drawing process on the structure and tensile properties of textile-grade PAN fiber and its carbon fiber

Authors
Lee, HwayoungLee, Lo-WoonLee, Seung-WookJoh, Han-IkJo, Seong-MuLee, Sungho
Issue Date
2014-05
Publisher
WALTER DE GRUYTER GMBH
Citation
E-POLYMERS, v.14, no.3
Abstract
Carbon fibers (CFs) were prepared using low-cost, textile-grade polyacrylonitrile fibers, which were 200% to 400% drawn in a hot water bath at 90 degrees C or/and in a tubular furnace at 180 degrees C. X-ray diffractograms confirmed that the drawing process led to higher crystallinity and molecular orientation. These fibers were stabilized in a convection oven at 25-255 degrees C for 390 min. After stabilization, carbonization was performed to obtain carbon fibers. The tensile strength of CFs without drawing was similar to 0.8 GPa; however, CFs with 200% and 200% drawing in a hot water bath at 90 degrees C and in a tubular furnace at 180 degrees C, respectively, showed a tensile strength of similar to 1.7 GPa. These results suggest that the drawing process of precursor fibers affected the tensile properties of the resulting CFs significantly.
Keywords
POLYACRYLONITRILE FIBERS; STABILIZATION; PRECURSOR; CARBONIZATION; POLYACRYLONITRILE FIBERS; STABILIZATION; PRECURSOR; CARBONIZATION; carbon fiber; drawing process; tensile properties; textile polyacrylonitrile; XRD
ISSN
1618-7229
URI
https://pubs.kist.re.kr/handle/201004/126847
DOI
10.1515/epoly-2013-0080
Appears in Collections:
KIST Article > 2014
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