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dc.contributor.authorKim, Chul Young-
dc.contributor.authorLee, Hee Ju-
dc.contributor.authorLee, Mi Kyeong-
dc.contributor.authorAhn, Mi-Jeong-
dc.contributor.authorKim, Jinwoong-
dc.date.accessioned2024-01-21T00:05:49Z-
dc.date.available2024-01-21T00:05:49Z-
dc.date.created2021-09-02-
dc.date.issued2007-11-
dc.identifier.issn1615-9306-
dc.identifier.urihttps://pubs.kist.re.kr/handle/201004/134014-
dc.description.abstractFlavanone glycosides were successfully separated from the crude extract of Poncirus trifoliata by preparative centrifugal partition chromatography with a two-phase solvent system composed of ethyl acetate - acetonitrile - water (3:2:5, v/v/v). Naringin (50.0 mg), neoponcirin (16.8 mg), and poncirin (71.9 mg) were purified from the 524 mg crude extract in only one step. The purities of the isolated compounds were determined to be over 90% by HPLC analysis and their structures were elucidated by H-1 NMR, C-13 NMR, and ESI-MS.-
dc.languageEnglish-
dc.publisherWILEY-V C H VERLAG GMBH-
dc.subjectPREPARATIVE ISOLATION-
dc.subjectFRUIT EXTRACT-
dc.subjectRAT-KIDNEY-
dc.subjectNARINGIN-
dc.subjectSEPARATION-
dc.subjectALKALOIDS-
dc.subjectDAMAGE-
dc.titleOne step purification of flavanone glycosides from Poncirus trifoliata by centrifugal partition chromatography-
dc.typeArticle-
dc.identifier.doi10.1002/jssc.200700168-
dc.description.journalClass1-
dc.identifier.bibliographicCitationJOURNAL OF SEPARATION SCIENCE, v.30, no.16, pp.2693 - 2697-
dc.citation.titleJOURNAL OF SEPARATION SCIENCE-
dc.citation.volume30-
dc.citation.number16-
dc.citation.startPage2693-
dc.citation.endPage2697-
dc.description.journalRegisteredClassscie-
dc.description.journalRegisteredClassscopus-
dc.identifier.wosid000250986700016-
dc.identifier.scopusid2-s2.0-36448944744-
dc.relation.journalWebOfScienceCategoryChemistry, Analytical-
dc.relation.journalResearchAreaChemistry-
dc.type.docTypeArticle-
dc.subject.keywordPlusPREPARATIVE ISOLATION-
dc.subject.keywordPlusFRUIT EXTRACT-
dc.subject.keywordPlusRAT-KIDNEY-
dc.subject.keywordPlusNARINGIN-
dc.subject.keywordPlusSEPARATION-
dc.subject.keywordPlusALKALOIDS-
dc.subject.keywordPlusDAMAGE-
dc.subject.keywordAuthorcentrifugal partition chromatography-
dc.subject.keywordAuthornaringin-
dc.subject.keywordAuthorneoponcirin-
dc.subject.keywordAuthorPoncirin-
dc.subject.keywordAuthorPoncirus trifoliata-
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